| 000 | 01970nam a22002777a 4500 | ||
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| 003 | ZW-GwMSU | ||
| 005 | 20250306083131.0 | ||
| 008 | 250306b |||||||| |||| 00| 0 eng d | ||
| 022 | _a09743626 | ||
| 040 |
_aMSU _bEnglish _cMSU _erda |
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| 050 | 0 | 0 | _aQD31 JOU |
| 100 | 1 |
_aSingh, Gurjaspreet _eauthor |
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| 245 | 1 | 0 |
_aSchiff bases of N-(2-aminoethyl)-3-aminopropyltrimethoxysilane and its silatranes: _bsynthesis and characterization / _ccreated by Gurjaspreet Singh, Amandeep Saroa, Sadhika Khullar, and Sanjay K. Mandal |
| 264 | 1 |
_aBangalore : _bSpringer, _c2015. |
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| 336 |
_2rdacontent _atext _btxt |
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| 337 |
_2rdamedia _aunmediated _bn |
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| 338 |
_2rdacarrier _avolume _bnc |
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| 440 |
_aJournal of chemical sciences _vVolume 127, number 4, |
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| 520 | 3 | _aThis paper aims at the introduction of azomethine group by the condensation reaction of N-(2-aminoethyl)-3-aminopropyltrimethoxysilane with different compounds containing carbonyl group such as 2’-hydroxyacetophenone, salicylaldehyde, pyrrole-2-carboxaldehyde, acetylacetone and ethyl acetoacetate. Further, transesterification reaction of these Schiff base modified silanes with triethanolamine as a tripodal ligand leads to the synthesis of corresponding silatranes 1–5 bearing Schiff base functionalized long chain in the axial position. All the synthesized compounds are characterized by spectroscopic methods, elemental analysis and mass spectrometry. The authentication of Schiff base modified silatranes is scrutinized by single X-ray crystal structure of silatrane 1. The thermal stability of the five silatranes is studied by thermo-gravimetric analysis (TGA). | |
| 650 |
_aSchiff base modified silane _vSchiff base modified silatranes _xN-(2-aminoethyl)-3-aminopropyltrimethoxysilane |
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| 700 | 1 |
_aSaroa, Amandeep _eco author |
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| 700 | 1 |
_aKhullar, Sadhika _eco author |
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| 700 | 1 |
_aMandal, Sanjay K. _eco author |
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| 856 | _uhttps://doi.org/10.1007/s12039-015-0822-1 | ||
| 942 |
_2lcc _cJA |
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| 999 |
_c169160 _d169160 |
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