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Green procedures for the chemoselective synthesis of acylals and their cleavage promoted by recoverable sulfonic acid based nanoporous carbon (CMK-5-SO3H) / created by Daryoush Zareyee, Ehsan Mirzajanzadeh and Mohammad Ali Khalilzadeh

By: Contributor(s): Material type: TextTextSeries: Journal of chemical sciences ; Volume 127, number 7,Bangalore : Springer, 2015Content type:
  • text
Media type:
  • unmediated
Carrier type:
  • volume
ISSN:
  • 09743626
Subject(s): LOC classification:
  • QD31 JOU
Online resources: Abstract: A selective synthesis of gem-diacetates from the reaction of aldehydes and acetic anhydride in the presence of recyclable nanoporous solid sulfonic acid (CMK-5-SO3H) under solvent-free reaction conditions is reported. The catalyst was also found to be highly active for deprotection of resulting acylals in water.
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Item type Current library Call number Vol info Status Notes Date due Barcode
Journal Article Journal Article Main Library - Special Collections QD31 JOU (Browse shelf(Opens below)) Vol. 127, no.7 (pages 1229-1234) Not for loan For in house use only

A selective synthesis of gem-diacetates from the reaction of aldehydes and acetic anhydride in the presence of recyclable nanoporous solid sulfonic acid (CMK-5-SO3H) under solvent-free reaction conditions is reported. The catalyst was also found to be highly active for deprotection of resulting acylals in water.

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