Green procedures for the chemoselective synthesis of acylals and their cleavage promoted by recoverable sulfonic acid based nanoporous carbon (CMK-5-SO3H) / created by Daryoush Zareyee, Ehsan Mirzajanzadeh and Mohammad Ali Khalilzadeh

By:

Zareyee, Daryoush [author]

Contributor(s):

Material type: Text

TextSeries: Journal of chemical sciences ; Volume 127, number 7,Bangalore : Springer, 2015Content type:

text

Media type:

unmediated

Carrier type:

volume

ISSN:

09743626

Subject(s):

1-Diacetates -- Acylals -- Solvent-free

LOC classification:

QD31 JOU

Online resources:

Click here to access online

Abstract: A selective synthesis of gem-diacetates from the reaction of aldehydes and acetic anhydride in the presence of recyclable nanoporous solid sulfonic acid (CMK-5-SO3H) under solvent-free reaction conditions is reported. The catalyst was also found to be highly active for deprotection of resulting acylals in water.

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Item type	Current library	Call number	Vol info	Status	Notes	Date due	Barcode
Journal Article	Main Library - Special Collections	QD31 JOU (Browse shelf(Opens below))	Vol. 127, no.7 (pages 1229-1234)	Not for loan	For in house use only

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A selective synthesis of gem-diacetates from the reaction of aldehydes and acetic anhydride in the presence of recyclable nanoporous solid sulfonic acid (CMK-5-SO3H) under solvent-free reaction conditions is reported. The catalyst was also found to be highly active for deprotection of resulting acylals in water.

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