MARC details
000 -LEADER |
fixed length control field |
02570nam a22003377a 4500 |
003 - CONTROL NUMBER IDENTIFIER |
control field |
ZW-GwMSU |
005 - DATE AND TIME OF LATEST TRANSACTION |
control field |
20250321070831.0 |
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
fixed length control field |
250321b |||||||| |||| 00| 0 eng d |
022 ## - INTERNATIONAL STANDARD SERIAL NUMBER |
International Standard Serial Number |
09743626 |
040 ## - CATALOGING SOURCE |
Original cataloging agency |
MSU |
Language of cataloging |
English |
Transcribing agency |
MSU |
Description conventions |
rda |
050 00 - LIBRARY OF CONGRESS CALL NUMBER |
Classification number |
QD31 JOU |
100 1# - MAIN ENTRY--PERSONAL NAME |
Personal name |
Tighadouini, Said |
Relator term |
author |
245 10 - TITLE STATEMENT |
Title |
Origin and switch of different colors : |
Remainder of title |
thermo-isomerism and crystal structure of (1E,2E)-bis[1-(4-nitrophenyl)ethylidene] hydrazine / |
Statement of responsibility, etc. |
created by Said Tighadouini, Smaail Radi, Loic Toupet, Muhammad Sirajuddin, Taibi Ben Hadda, Mehmet Akkurt, Ismail Warad, Yahia N. Mabkhot and Saqib Ali |
264 1# - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE |
Place of production, publication, distribution, manufacture |
Bangalore : |
Name of producer, publisher, distributor, manufacturer |
Springer, |
Date of production, publication, distribution, manufacture, or copyright notice |
2015. |
336 ## - CONTENT TYPE |
Source |
rdacontent |
Content type term |
text |
Content type code |
txt |
337 ## - MEDIA TYPE |
Source |
rdamedia |
Media type term |
unmediated |
Media type code |
n |
338 ## - CARRIER TYPE |
Source |
rdacarrier |
Carrier type term |
volume |
Carrier type code |
nc |
440 ## - SERIES STATEMENT/ADDED ENTRY--TITLE |
Title |
Journal of chemical sciences |
Volume/sequential designation |
Volume 127, number 12, |
520 3# - SUMMARY, ETC. |
Summary, etc. |
A new symmetric branched 4-nitrophenyl hydrazine compound has been prepared in one-step procedure by direct condensation of aromatic ketone with hydrazine in MeOH. The synthesized compound, red isomer, was characterized by IR, 1H and 13C NMR spectroscopy, Elemental analyses, Mass spectrometry and X-ray crystallography. Refluxing in MeOH solution led to thermo-isomerism offering a white isomer product that was characterized by X-ray crystallography. The red isomer crystallizes in the orthorhombic system having space group Pbcn, with a = 12.7612(4), b = 11.5197(3), c = 20.1586(7) Å, V = 2963.42(16) Å 3, Z = 8 while the white isomer crystallizes in the triclinic system having space group P −1, with a = 7.8007(4), 8.5966(7), 12.224 (1) Å, α= 71.133(7), β= 81.281(5), γ= 74.895(5) ∘, V = 746.86(9) Å 3, Z = 2. Molecules of both compounds are twisted at N2–N3 bond with the C7-N2-N3-C9 torsion angle of 155.23(12) and −113.36(18) ∘, respectively. The crystal structures of both compounds are stabilized by weak intramolecular C—H …N contacts and intermolecular C—H …O hydrogen bonding interactions. In addition, π– π stacking interactions are observed between the same aromatic rings of molecules. |
650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM |
Topical term or geographic name entry element |
Hydrazine derivative |
Form subdivision |
Crystal structure |
General subdivision |
Thermo-isomerism |
700 1# - ADDED ENTRY--PERSONAL NAME |
Personal name |
Radi, Smaail |
Relator term |
co author |
700 1# - ADDED ENTRY--PERSONAL NAME |
Personal name |
Toupet, Loic |
Relator term |
co author |
700 1# - ADDED ENTRY--PERSONAL NAME |
Personal name |
Sirajuddin, Muhammad |
Relator term |
co author |
700 1# - ADDED ENTRY--PERSONAL NAME |
Personal name |
Hadda, Taibi Ben |
Relator term |
co author |
700 1# - ADDED ENTRY--PERSONAL NAME |
Personal name |
Akkurt, Mehmet |
Relator term |
co author |
700 1# - ADDED ENTRY--PERSONAL NAME |
Personal name |
Warad, Ismail |
Relator term |
co author |
700 1# - ADDED ENTRY--PERSONAL NAME |
Personal name |
Mabkhot, Yahia N. |
Relator term |
co author |
700 1# - ADDED ENTRY--PERSONAL NAME |
Personal name |
Ali, Saqib |
Relator term |
co author |
856 ## - ELECTRONIC LOCATION AND ACCESS |
Uniform Resource Identifier |
https://doi.org/10.1007/s12039-015-0992-x |
942 ## - ADDED ENTRY ELEMENTS (KOHA) |
Source of classification or shelving scheme |
Library of Congress Classification |
Koha item type |
Journal Article |